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ACADEMIC YEAR: 2019-2020

COURSE:: CHIMICA ANALITICA TYPE OF EDUCATIONAL ACTIVITY: Fundamental TEACHER: Prof. Dr. Antonio Guerrieri

e-mail: [email protected] Web site:

http://docenti.unibas.it/site/home/docente.html?m=000966

phone: 0971/205460 mobile:

Language: ITALIANO ETCS: 12

(8 lessons /4 practical lab activities)

n. of hours: 112

(64 for lessons and 48 for practical lab activities)

Campus: Potenza

Dept/School: Dipartimento di Scienze

CdS: Laurea in Biotecnologie (L2)

Semester: annual (tentatively from 1/10/2019 to 31/05/2020-

20/06/2020) EDUCATIONAL GOALS AND EXPECTED LEARNING OUTCOMES

o Knowledge and understanding: the student should demonstrate to know and understand the fundamental notions of analytical chemistry and the fundamental knowledge on the most common analytical instrumentation.

o Ability to apply knowledge and understanding: the student should demonstrate to be able to face the most common analytical problems as well as the use of the most common analytical instrumentation.

o Autonomy of judgment: the student should demonstrate to be able to make an independent judgment using the basic knowledge learned from the subject.

o Communication skills: the student should have the ability to summarize and explain using the terminology of the subject.

o Learning skills: the student should be able to understand publications and follow in-depth courses, specialized seminars and masters.

PRE-REQUIREMENTS

o attendance of lectures: HIGLY suggested o attendance of lab activities: COMPULSORY

o preparatory exams: Istituzioni di Matematica, Fisica, Chimica generale e inorganica SYLLABUS

Analytical Chemistry: an introduction.

Statistical data treatment and processing.

Equilibria in aqueous solutions for acids, bases, salts and buffers.

Titrations.

Electrochemical reactions and equilibria.

Potentiometry. pHmeters. Ion selective electrodes.

Spectroscopy. Emission. Absorption. Fluorescence.

Instrumentation in spectroscopy.

Lab activities

 The analytical approaches in lab

 Titration of HCl

 Titration of NaOH

 Determination of acetic acid in commercial vinegars by titration

 Deyermination of citric acid in lemon juices by titration

 The pH meter

 Potentiometric titrations

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 Spectrophotometry with Lambert Beer applications to cytochrome c determination

TEACHING METHODS

o The course includes 112 hours of teaching between lessons and laboratory. In particular, 64 hours of classroom lessons and 48 hours of laboratory exercises are planned.

EVALUATION METHODS

o Final oral exam to ascertain the actual acquisition by the student of the knowledge and skills described in the section " EDUCATIONAL GOALS AND EXPECTED LEARNING OUTCOMES " and discussion of reports on laboratory exercises.

o

The final evaluation will be expressed with a mark of thirty and possible praise.

TEXBOOKS AND ON-LINE EDUCATIONAL MATERIALS o lecture notes; lesson slides; lab activity notes

o Suggested Texbooks

Title:Fondamenti di chimica analitica

Authors:Skoog Douglas A.,West Donald M.,Holler James F.

Editor:Edises

Publication date:1998 ISBN:887959138X ISBN-13:9788879591386

Title:Chimica analitica strumentale

Authors:Skoog Douglas A.,West Donald M.

Editor:Edises

Publication Date:1995

ISBN:8879590669

ISBN-13:9788879590662

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INTERACTION WITH STUDENT

Conventional approaches (e.g. student welcome) as well as internet ones (e.g. email) for discussions and deepening of lectures and lab activities .

TIMETABLE FOR STUDENT WELCOME

DAY FROM TO LOCATION

MONDAY 17.30 20.30 Professor Office

TUESDAY 17.30 20.30 Professor Office

WEDSNEDAY 18.00 20.30 Professor Office

THURSDAY 15.00 18.00 Professor Office

CALLS FOR EXAMINATION (exact dates to be defined)1

Month Year Expected call

February 2020 18

March 2020 17

June 2020 23

July 2020 14

September 2020 22

October 2020 20

December 2020 15

EXAMINATION PANEL:

President: prof. dr. Antonio Guerrieri Member: prof.ssa Anna Maria Salvi Member: dr.ssa Rosanna Ciriello Member: dr.ssa Giuliana Bianco Member: dr. Fausto Langerame

SEMINARS BY EXTERNAL EXPERTS YES □ NO 

ALTRE INFORMAZIONI

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