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9

th

European Conference on Wood Modification

ECWM9

September 17 and 18, 2018, Arnhem, The Netherlands

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BOOK OF ABSTRACTS

9

th

European Conference on Wood Modification

Arnhem, The Netherlands

17-18 September 2018

In association with:

COST FP1407 ModWoodLife

Edited by:

Jos Creemers, Thomas Houben, Bôke Tjeerdsma, Holger Militz

and Brigitte Junge

Secretariat:

SHR B.V.

Nieuwe Kanaal 9b

6709 PA Wageningen

www.ecwm9.shr.nl

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BOOK OF ABSTRACTS

Legal Notice

Although all reasonable efforts were made by the editorial team to ensure the scientific quality of the contents of these conference proceedings, the final responsibility for the contents of individual articles therein remains with the respective authors. The editors accept no responsibility for the information contained herein. The inclusion of information in this publication does not constitute any form of endorsement by the editors. The editorial team is not responsible for the contents of external websites referred to in this publication.

No permission is required to reproduce or utilise the contents of these abstracts other than in the case of diagrams, images, or other material from other copyright holders. In such cases the permission of the original copyright holder must be obtained. The abstracts may be sited as Abstracts of the 9th European Conference on Wood Modification 2018, Arnhem, The

Netherlands.

Copyright © SHR B.V.

Nieuwe Kanaal 9b, 6709 PA Wageningen, The Netherlands

www.shr.nl

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3

Preface

SHR was one of the first research institutes in Europe, who already in the 1990´s did substantial research work to develop wood modification processes. It appeared, that this research area was very complex, and that for a successful application of potential processes needed

outcomes of this EU financed network. Since than, ECWM´s were held each 2-3 years at different places around Europe, and now we can celebrate the 9th ECWM in the Netherlands,

organized by SHR where it all began.

As already before, ECWM 9 is linked up to the European COST organisation. Thanks to the COST Action FP 1407 ModWoodLife to join and strengthen our network!

The participation of researchers of all around the world make it obvious that the name

and academia from Europe and abroad! This success has led, once again, to a large number of abstracts submitted to the organizers. In general, these abstracts were of a high quality and the members of the Scientific Committee had a hard time to select 44 full presentations and 50 poster presentations out of the many applications. We hope we have found the right balance between scientific and applied presentations to reach the key goal of ECWM: to attract researchers from academia and industry to join their expertises in this very exciting research

The local conference organizers from SHR have done a great job this past year to make us feel welcome in The Netherlands and to let the conference be a success. Thank you very much to Bôke and team!

Prof. Dr. Holger Militz

Chairman of Scientific Committee

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Scientific Committee

Dr. Julia Milne e Carmo, Carmo Group, Portugal

Prof. Dr. Callum Hill, JCH Industrial Ecology Ltd., United Kingdom Dr. Dennis Jones, Timber Consultancy (UK) / LTU, Sweden

Prof. Dr. Holger Militz, Göttingen Uni., Germany (Chairman of Scientific Committee) Mr. Jos Creemers, SHR, The Netherlands

Mr. Bôke Tjeerdsma, SHR, The Netherlands Prof. Dr. Joris Van Acker, Ghent Uni., Belgium

Dr. Andreja Kutnar, University of Primorska, Slovenia (FP 1407)

Local Organising Committee

Mr. Bôke Tjeerdsma, SHR; The Netherlands (Chairman of Organizing Committee) Mrs. Marina van der Zee, SHR; The Netherlands

Mr. Jos Creemers, SHR SHR; The Netherlands Dr. René Klaassen,SHR SHR; The Netherlands Mr. Bas Holleboom, SKH SKH; The Netherlands Mrs. Mariena Mooi, SHR SHR; The Netherlands Mrs. Jos Gootjes, SHR SHR; The Netherlands

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5

Wood modification in practice

The European Conference on Wood Modification takes place on the 17th and 18th of

September 2018 in Arnhem, The Netherlands and is organised by SHR. At this conference researchers and people from industry from all over the world will come together to share their knowledge and experiences with the latest developments on wood modification methods,

and still play in the development and industrial application of modified wood.

Techniques and methods designed for improving wood properties are almost as old as mankind itself. However the scientific and industrial rise of wood modification became significant under the influence of a number of social and economic developments in the eighties and nineties of the previous century. A strong need was felt to find alternatives for the use of tropical hardwoods and preservative treated wood, which were both under pressure for a variety of reasons. The discussions regarding a clean environment, sustainable forest management, wood use and the increasing wood demands from emerging markets in Asia also had a big impact. Wood modification was recognized to have the ability to offer a more, better and sustainable way of making use of wood as a durable material in a broad range of applications. Besides that, it was found to be a supreme method for upgrading the properties of lesser used timber species and to provide technical solutions to overcome some of the natural deficiencies of wood as water uptake, decay and dimensional changes.

Over the last decades an enormous amount of scientific work has been performed and published. We have seen many innovative modification ideas, methods and techniques

, ideas need to be developed further and put into practice. We are proud that in The Netherlands we have created a setting with a high level of knowledge, innovative thinking combined with entrepreneurship, which lead to a variety of flourishing companies involved in industrial production of modified wood. Not only producing companies, but also the wood processing industry has adopted modified wood as a highly appreciated durable material. We can declare that modified wood has become a lasting factor in the wood processing industry.

For these reasons SHR and we as the organising team, are excited to welcome you all here in The Netherlands for the 9th European Conference on Wood Modification. We hope you will

enjoy your stay here in Arnhem and become inspired by all attendees, presenters and new insights this conference has to offer.

Welcome!

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COST 1407 - Foreword

integrated scientific and environment

European Conference of Wood Modification. The conference brings together researchers from across Europe and beyond that jointly are addressing the mounting pressure on renewable resources (as a material source, for recreational, ecological, and other uses). By maximising the efficiency of materials derived from them, the wood modification community plays an important role. The efficiency can only be achieved if new methods to improve the functionality, durability, properties, and environmental impacts will be developed. Wood modification addresses these requirements directly, allowing wood to be used in more applications, including increased use of under-utilised species. Wood modification also addresses undesirable characteristics of wood such as fungal resistance, UV-stability, and moisture sensitivity. The COST Action FP1407 has been successful in addressing these needs in the past 3 years. We are in the last year of the Action and therefore it is even more

important for us to be at ECWM9. Only sustainable collaboration and joint efforts will deliver the impacts. That objective of the Action FP1407, to characterise the relationship between wood modification processing, product properties, and the associated environmental impacts in order to maximise sustainability and minimize environmental impacts, has great value for the forest sector, for researchers, and society at large.

Wishing you a successful and memorable conference full of fruitful discussions.

Andreja Kutnar Chair, COST FP1407

Denis Jones

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Table of Contents

7

Table of Contents

Session One: Wood Modification World-wide -

keynote presentations

Modified wood in circular economy a critical review

Henrik Heräjärvi, Janni Kunttu, Elias Hurmekoski, Teppo Hujala

17

A review of wood modification across Europe as part of COST FP1407 Dennis Jones, Dick Sandberg, Andreja Kutnar

18

What is wrong with Wood Modification in the U.S.? Jeffrey Morrell

19

Wood Chemical Modification in China 20 Zefang Xiao, Qingwen Wan, Jian Li, and Yanjun Xie

Session Two: Commercial and Market Opportunities for Modified

Wood

New Standards for Approval of Modified Wood within the Nordic Wood Preservation Council (NWPC)

Niels Morsing, Søren Bang-Achton, Emil Engelund Thybring, Morten Klamer

25

Kebony Clear Produced in Belgium

Per Brynildsen, Omar Roels, Bruno Van den Branden

26

Improved dimensional stability of polypyrrole enriched spruce as an indication for chemical change

Andries van Eckeveld, Rabi Malki, Michael Sailer, Jacco Eversdijk

27

Practical experience of acetylated wood fibre panel products in Dutch door manufacturing

Jeroen Lückers

28

Wood Modification with DMDHEU (1.3-dimethylol-4.5-dihydroxy-ethyleneurea) Status quo and latest research activities

Lukas Emmerich, Holger Militz

29

Architects perception of modified wood: a parallel study in selected countries of Europe

Manja Kitek Kuzman, Eva Haviarova, Dick Sandberg

30

Enhancing the Properties of ThermoWood® with Phenolic Resin Treatment

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Table of Contents

Session Three: Poster Session 1

Effect of Thermo-Mechanical Treatment on Properties of Parica Laminated Veneer Lumber (Schizolobium amazonicum Huber ex Ducke)

Mírian de Almeida Costa, Cláudio Henrique Soares Del Menezzi

35

TanWood®: The Brazilian Process of Thermal Modification of Wood Leonardo Puppi Bernardi, Djeison Cesar Batista

36

Examining the coating performance of finishes on acetylated hornbeam wood (Carpinus betulus L.)

Fanni Fodor, Róbert Németh

37

Colour response of heat treated spruce and pine with different surface coatings in outdoor exposure

Niclas Björngrim, Marie Hartwig, Olle Hagman, Tom Morén

38

New substrates for wood modification. Characterising pore size distributions in variously dried softwood

Warren Grigsby, Elizabeth Dunningham, Hank Kroese

39

Determination of resistance of thermally treated wood to weather conditions in different countries (HTW) - Preliminary results

Idalina Domingos, José Ferreira, Luisa Cruz-Lopes, Júlia Carmo, Jorge Martins, René Herrer, Lina Nunes, Bruno Esteves

40

Investigation of Abies alba wood thermal stability according to its radial position Joël Hamada, Anélie Pétrissans, Julien Ruell, Frédéric Mothe,, Francis Colin, Mathieu Pétrissan, Philippe Gérardin

41

Properties improvement of bamboo materials through furfurylation Li Wanju, Wang Hankun, Liu Minghui, Yu Yan

42

Veneer modification with fire retardant chemicals

Saara Hautamäki, Michael Altgen, Tuomas Hänninen, Lauri Rautkari

43

Natural Weathering and Photostability of Wood Modified by Fatty Acid esters Mohamed Jebrane, Nasko Terziev, Ivo Heinemaa

44

Effects of thermal modification on bending properties and chemical structure of Iroko and Padauk

Michal Kroupa, Milan Gaff, Olov Karlsson, Olena Myronycheva, Dick Sandberg

45

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Table of Contents

9 Water free PEG impregnation of hardwood veneer using a roll press

Tillmann Meints, Axel Rindler, Niklas Bugelnig, Christian Hansmann

48

The impact of cerium dioxide nanoparticles on thermally modified wood-coating system during weathering

-49

Application of time-temperature-humidity superposition to the hygrothermally accelerated ageing of spruce wood

Eiichi Obataya, Nanami Zeniya, Kaoru Endo, Miyuki Matsuo-Ueda

50

Preliminary studies on the effect of acetylation and subsequent weathering on tensile strength and stiffness of Rubber wood (Hevea brasiliensis)

Samuel Olaniran, E. Cabane, M. Rüggeberg

51

Mild torrefaction pre-treatment of eucalypts aiming at its energetic valorisation Solange de Oliveira Araújo, Duarte M. Neiva, Angélica de Cássia Carneiro, Bruno Esteves, Jorge Gominho, Helena Pereira

52

Influence of various polyethylene glycol treatments on the dimensional stability of beech wood.

Sabrina Puttmann, Lukan Müller, Bertil Burian, Marcus Müller

53

Adhesion of coatings to plasma modified wood at accelerated weathering Ladislav Reinprecht,

54

Measuring Accessibility of OH groups in Scots Pine with Dynamic Vapour Sorption Apparatus

Tuuli Uimonen, Saara Hautamäki, Maija Kymäläinen, Lauri Raukari

55

Plasma treatment of wood veneers: a review

Richard Wascher, Georg Avramidis, Holger Militz, Wolfgang Viöl

56

Saturated gaseous ammonia treatment for improved densification of beech wood Sorption and mechanical properties

Mario Zauer, Tobias Dietrich, Herwig Hackenberg, André Wagenführ

57

Natural surface ageing affects bonding quality of thermally modified wood , Goran Mihulja and Gustav Gabrek

55

Session 4A: Properties 1

The potential for use of acetylated wood in musical instruments making Stergios Adamopoulos, Sheikh Ali Ahmed, Chiel Lankveld

61

Influence on acoustical properties of resonant soundboard material through different processes of thermal modification

David Zerbst, Lothar Clauder, Dave Olson, Alexander Pfriem

62

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Table of Contents

Measuring the Free Hydroxyl Content in Wood Modified by Acetic or Propionic Anhydride

Callum Hill, Greeley Beck, Erik Larnøy, Sarah Strohbusch, Holger Militz

63

Pre-treatment with Ionic Liquids or Organic Superbases to Reduce Spring-Back and Set-Recovery of Surface-Densified Scots pine

Benedikt Neyses, Olov Karlsson, Dick Sandberg

64

Potential solutions for gluing acetylated wood in load bearing constructions Andreas Treu, Ronny Bredsen, Ferry Bongers

65

Combustion behaviour of wood chemically modified with DMDHEU-, PF-, and MF-resins

Zhijun Zhang, Zefang Xiao, Holger Militz, Carsten Mai, Yanjun Xie

66

Session 4B: Thermal Modification

Potential to limit variation in durability of thermally modified timber Joris van Acker, Jan Van Den Bulcke

69

Thermovuoto thermal modification of eight European wood species

Ignazia Cuccui, Nasko Terziev, Giovanna Bochicchio, Ottaviano Allegretti

70

Differences in the mechanical behaviour of wood after thermal modification in oven-dry or water-saturated state

Michael Altgen, Tuuli Uimonen, Lauri Rautkari

71

Thermal modification of wax impregnated wood Miha Humar,

72

The role of accessible hydroxyl groups in reversible and irreversible EMC changes by thermal wood modification

Wim Willems, Michael Altgen, Lauri Rautkari

73

Session 5: COST FP 1407

Wood Furfurylation as a way to valorise European Beech and promote Circular and Bio-Economy

Christine Gérardin, Aurélia Imbert, Prabu Satria Sejati, Emmanuel Fredon,

Stéphane Dumarçay, Eric Masson, Arnaud Besserer, Benoit Laibe, Rémi Laibe, Hugo Sellier, Philippe Gérardin

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Table of Contents

11 Perception and evaluation of modified wood

Dean Lipovac, Michael D. Burnard, Andreja Kutnar

79

Valorization of Beech Wood through Development of Innovative Friendly Environmentally Chemical Modification Treatments

Mahdi Mubarok, Stéphane Dumarcay, Holger Militz, Philippe Gérardin

80

Infrared spectroscopy and chemometric methods for the evaluation of the thermal/chemical treatment effectiveness of hardwoods

Carmen Mihaela Popescu,

Maria-Cristina Popescu, Dennis Jones

81

Performance of modified wood in service multi-sensor and multi-scale evaluation Anna Sandak, Jakub Sandak, Marta Petrillo, Paolo Grossi

82

Carbon footprint of decking materials- a comparison of modified wood and preservative treated wood

Lars Tellnes, Gry Alfredsen, Per Otto Flæte, Lone Ross Gobakken

83

Session Six A: Properties 2

Strength classification of acetylated radiata pine Ferry Bongers, John Alexander

87

Effect of DMDHEU modification on physical and mechanical properties of top-layer lamellas for multi-layer parquet flooring

Lukas Emmerich, Holger Militz

88

Cutting forces when machining thermally modified poplar preliminary results Giacomo Goli, Rémi Curti, Bertrand Marcon, Antonio Scippa, Marco Fioravanti, Gianni Campatelli, Louis Denaud

89

Properties of MMA treated thermally modified Norway spruce wood 90

Differential expression of Postia placenta wood decay genes in modified wood Rebecka Ringman, Annica Pilgård, Martina Kölle, Klaus Richter

91

Session Six B: Chemical Modification

Suitability of Lignin-Derived Monophenols to Replace Phenol in Phenol-Formaldehyde Resin for the Use in Wood Treatment

Vladimirs Biziks, Marco Fleckenstein, Carsten Mai, Holger Militz

95

A new method of wood protection by chemical modification with polyglycerol succinate copolymer

Emmanuel Fredon, Marie France Thevenon, Philippe Gérardin

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Table of Contents

The effect of humidity and temperature on the dynamic-mechanical behaviour of phenol-formaldehyde impregnated beech wood veneer

Leo Felix Munier, Tom Franke, Nadine Herold, Alexander Pfriem

97

Biopolyesters for wood modification: technical validation towards implementation Marion Noël, Charlotte Grosse, Ingunn Burud, Marie-France Thévenon,

Philippe Gérardin

98

The Maillard reaction for wood modification: The influence of reagent

concentrations, reaction temperature and soaking time on the leachability and cell wall penetration of reagents

Kelly Peeters,

99

Session Seven: Poster Session 2

Wood thermal modification and impregnation: some aspects of double treatment Bruno Andersons, ndersone,

103

Hydrophobisation of hardwood surfaces by means of environmentally-friendly fine wax particles

Benjamin Arminger, Wolfgang Gindl-Altmutter, Christian Hansmann

104

Further Treatment Option after Longitudinal Wood Compression Mátyás Báder, Róbert Németh

105

Effect of combined modification processes on the physical properties of wood Miklós Bak, Róbert Németh, Norbert Kelemen

106

Bending properties and strain fields around knots in thermally modified timber Joran van Blokland, Stergios Adamopoulos, Anders Olsson,

Jan Oscarsson

107

Thermomechanical (TM) treatment of beech wood (Fagus sylvatica L.) to substitute Indian rosewood (Dalbergia latifolia ROXB.) in musical instruments - mechanical and acoustic properties

Tobias Dietrich, Dr. Mario Zauer, Robert Krüge, Prof. Dr. André Wagenführ

108

Colour Stability Testing: Comparison of test methods Rosie Sargent and Elizabeth Dunningham

109

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Table of Contents

13 Investigation of Birch Wood Impregnation with Phenol-Formaldehyde (PF) Resins

Juris Grinins, Ilze Irbe, Vladimirs Biziks, Janis Rizikovs, Sascha Bicke, Holger Militz

112

Thermal properties and density profile of poplar wood (Populus nigra L.) thermally and thermo-mechanically modified

113

Water sorption properties of surface charred wood Maija Kymäläinen, Saara Hautamäki, Lauri Raukari

114

Energy dispersive x-ray fluorescence (ED-XRF) for the multi-elemental analysis of thermally modified wood treated with coatings systems

René Herrera Díaz, Marco Fellin, Martino Negri, Jalel Labidi

115

Thermowood® vs Termovuoto process comparison of thermally modified timber in industrial conditions

Mohamed Jebrane, Ignazia Cuccui, Ottaviano Allegretti, Ernesto Uetimane Jr., Nasko Terziev

116

Study on Drying Characteristics of Poplar Wood Impregnated with Urea- formaldehyde Resin

Yang Lihu, Yuan Haiguang

117

Life cycle assessment of bio-based façades during and after service life: maintenance planning and re-use

Marta Petrillo, Jakub Jakub, Anna Sandak, Paolo Grossi, Andreja Kutnar

118

Raman spectral imaging of chemically modified Scots pine

Carmen Mihaela Popescu, Lauri Rautkari, Michael Altgen, Tiina Belt, Mikko Mäkelä

119

Changes in longitudinal modulus of elasticity of Douglas-fir during low temperature thermal treatment

Dan Ridley-Ellis, Carmen-Mihaela Popescu

120

Investigation of the effect of moderate heat treatment on wood hygroscopicity by NMR relaxometry

Leila Rostom, Denis Courtier-Murias, Stéphane Rodts, Sabine Caré

121

Effect of wood modification and weathering progress on the radiation emissivity Anna Sandak, Jakub Sandak, Marta Petrillo, Paolo Grossi

122

Composition of monosaccharides in aqueous extracts from thermally modified wood Ekaterina Sidorova, Olov Karlsson, Dick Sandberg

123

Insights into stability of glued joints between thermally modified timber: adaptation of an artificial weathering test

Morwenna Spear, Raisa Teciu, Graham Ormondroyd

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Table of Contents

Water resistant tannin polymers Gianluca Tondi, Lukas Sommerauer

125

Dynamic and static mechanical properties of thermally modified Eucalyptus nitens in an open and closed reactor system

Maximilian Wentzel, Christian Brischke, Holger Militz

126

Session 8: Performance

Enhancing the material properties of wood through furfurylation

Wanju Li, Changhua Fang, Hankun Wang, Xuexia Zhang, Dan Ren, Yan Yu

129

Comparative studies on the biological durability of identical thermally modified wood from field and laboratory tests

Sven Hertrich, Lothar Clauder, Silte Lautner, Alexander Pfriem

130

Appearance of solid wood decking: requirements and assessment Wolfram Scheiding, Philipp Flade, Katharina Plaschkies, Björn Weiß

131

Monitoring the performance of Accoya in different applications René Klaassen, Bôke Tjeerdsma, René Hillebrink

132

Performance of chemically modified wood under marine conditions during nine years of exposure

Christian Brischke, Antje Gellerich, André Klüppel, Holger Militz

133

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European Conference on Wood Modification 2018

Cutting forces when machining thermally modified poplar –

preliminary results

Giacomo Goli

1

, Rémi Curti

2

, Bertrand Marcon

2

, Antonio Scippa

3

, Marco

Fioravanti

1

, Gianni Campatelli

3

, Louis Denaud

2

1GESAAF - University of Florence, Via S. Bonaventura 13, IT-50145, Florence [email:

giacomo.goli@unifi.it – marco.fioravanti@unifi.it]

2LaBoMaP – Arts et Métiers Paristech, Rue porte de Paris, FR-71250 Cluny [email:

remi.curti@ensam.eu, bertrand.marcon@ensam.eu, louis.denaud@ensam.eu]

3 DIEF - University of Florence, Via Santa Marta 3, IT-50139, Florence [email: antonio.scippa@unifi.it –

gianni.campatelli@unifi.it]

Keywords: cutting forces, grain orientation, poplar wood, thermal modification

ABSTRACT

This work explores the possibility, with a simple and innovative procedure, to assess the machining properties of thermally modified wood for a whole set of grain orientations and compare the results with unmodified wood. An experimental test set up was designed, few exploratory tests performed and a data analysis procedure developed. This method has shown to work fine to describe and compare the cutting forces of unmodified and thermally modified wood at different grains orientations. With a simple test a whole set of grain orientations can be acquired and with few tests performed at different depths of cut it is possible to evaluate the specific cutting forces. The forces when machining unmodified and thermally modified wood have shown to be very similar when machining along the grain. However, the cutting forces when machining thermally modified wood with or against the grain have shown to be lower than for untreated wood. The data analysis method, actually based on filtering the signals that are strongly affected by the system dynamical excitation, should be improved in order to calculate the real cutting forces acting.

INTRODUCTION

The use of thermally modified wood is getting more and more frequent in different uses such as: internal furniture for its dark colour, in use in wet conditions, external use where durability and hygroscopic stability are needed. It is also getting easier and easier to find this product on the market. Even if thermally modified wood is not a new product, the efforts of researchers until now have been focused mainly on treatment processes, chemical analysis, durability, dimensional stability, and mechanical performances. The machining of modified wood is something not very explored yet. Some information about handling, machining and gluing of this material can be found on (Finnish ThermoWood Association 2003). The quality after machining has also been assessed by different authors such as (de Moura et al. 2011; Budakçı et al. 2013; de Moura Palermo et al. 2014; Tu et al. 2014; Palermo Pires De Moura et al. 2015; Sandak et al. 2017). The cutting forces as well as the specific cutting coefficients are not investigated yet. In this article, the general approach described in (Goli and Sandak 2016) was used for the machining of unmodified and thermally modified poplar wood disks. The same disk (one for thermally modified wood and one for unmodified wood) was machined with different depths of cut (0.3, 0.7, 1.1, 1.5 mm) and the forces measured on two horizontal orthogonal directions (X, Y) in order to assess the cutting forces when machining with different depths of cut

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European Conference on Wood Modification 2018

and grain orientations. This work is not meant to give extensive information on cutting forces and to precisely assess the specific cutting coefficients; but the aim is to explore the possibility to assess the machining properties of thermally modified wood at a whole set of grain orientation, compared to unmodified wood using an innovative and rapid procedure.

EXPERIMENTAL

Two boards of unmodified and thermally modified poplar wood (Populus sp.) were machined into a disk shape. Afterward, the disk was stiffly screwed on a Kistler 9255 type tri-axial piezoelectric dynamometric platform for the measurement of the cutting forces. The platform was driven by a Kistler type 5019 charge amplifier set with 100 N.V-1 and “Long” time constant mode. The tests on the disks were done with a low-pass filter with a cut-off frequency of 10 kHz in order to avoid aliasing. The disk was machined using a SCM Record 1 3-axis CNC centre. The machining was done by a single straight blade balanced tool in order to get an invariant chip thickness.

a b

Figure 1: Experimental set up of the wood disks screwed on the dynamometric platform. a) untreated poplar and b)thermally modified poplar.

The diameter of the tool was 80 mm and the blade was a tungsten carbide freshly sharpened insert with a rake angle of 25° and a blade angle of 55°. The spindle was set to rotate at 3000 rpm both for measurement and preparatory cut. For every depth of cut the surface was prepared before the measurement by machining 0.2 mm of depth of cut in 5 successive steps with a feeding speed of 1 m.min-1. The measurement of the cutting forces was done after surface preparation, machining with up-milling technique and with a feeding speed of 3 m.min-1. The analogue outputs of the charge amplifiers were acquired

synchronously with a sampling frequency of 50 kHz by a 16 bits National Instrument acquisition board model NI-9215 installed on a USB chassis model cDAQ-9174. The different channels were acquired by DASYLab® software and analysed with MATLAB®. Wood was machined after a stabilizing period in internal environment with a moisture content of 7.8% for untreated one and 6.4% for thermally modified one. The density at standard environmental conditions (20 °C @ 65% relative humidity) was determined to be 330 kg.m-3 and 340 kg.m-3for for untreated and thermally modified wood respectively. Thermally modified poplar was treated at 215 °C using the ThermoWood® process. The rough signals obtained machining a disk are shown in Figure 2a for X- and

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European Conference on Wood Modification 2018

rough force could include relevant information of the acting process, the signals were low-pass filtered with a cutting frequency of 200 Hz. The result of the filtering is shown in Figure 2b. As it can be observed, a large part of the free vibration is removed. The values of forces obtained with this procedure were then plotted as absolute values versus the angular position for the X-axis (Figure 2c) and for the Y-axis (Figure 2d) and the envelope extracted through a Matlab® code. Both graphs present two symmetric parts corresponding to first and second half of the disk. The X- and Y-axis envelope values were then used to calculate the resulting force as sum of vectors, as reported in Figure 2e. Because the disk is made of two equal halves (axially symmetric regarding the grain orientation), the resulting force was computed as the average of these two halves (Figure 2f).

a b

C d

e f

Figure 2: These graphs are obtained by processing the test performed on thermally modified poplar wood machining with a depth of cut of 1.1 mm. a) Rough forces vs number of samples, b) 200 Hz

low-pass filtered cutting forces vs. number of samples, c) Force on the X-axis with its envelope vs the angular position, d) Force on the Y-axis and its envelope vs. angular position, e) Resulting force calculated as vectors sum of X- and Y-axis components vs. angular position, and f) Resulting force is

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European Conference on Wood Modification 2018

To summarize, this simple data processing doesn’t allowed to obtain the true values of cutting forces, but at least to make a first assessment of the possibility to make comparisons unmodified and thermally modified wood. The same procedure could ba applied to different materials, using different tools etc.

RESULTS AND DISCUSSION

The data obtained applying the above presented method when machining unmodified and thermally modified wood are shown in Figure 3. The continuous line indicates unmodified wood while dashed line indicates thermally modified wood. In blue are shown the cutting forces when machining at 0.3 mm of depth of cut (DOC), in red when machining with 0.7 mm DOC, and in orange when machining with 1.1 mm DOC.

Figure 3: Filtered cutting forces normalized by the engaged blade length when machining unmodified (continuous line) and thermally modified (dashed line) wood. In the lower part with a depth of cut

(DOC) of 0.3 mm, in the upper part of 1.1 mm and in the middle of 0.7 mm.

It can observe, as expected, a clear trend of increased cutting forces with increasing both for unmodified and thermally modified wood. A clear difference in cutting forces related to wood anisotropy can also be observed when machining at different angular positions. The minimum force is reached when machining along the grain (angular position 90°) while the maximum is got when machining against the grain (angular position between 14 and 160°). These results are coherent with previous investigations conducted on maple (Costes et al. 2004) and Douglas fir (Goli et al. 2010). Repeatable trends between

0.3 mm DOC 1.1 mm DOC

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European Conference on Wood Modification 2018

hand, while machining with or against the grain, thermally modified wood shows much lower cutting forces compared to unmodified wood.

CONCLUSIONS

The proposed experimental set up has shown to work fine even if at present the data analysis should be improved. The use of filtering at the beginning of the data treatment allows to compare cutting forces while machining modified and unmodified wood and to investigate the impact of grain orientation. The method is proved to be relevant to study the impact of thermal modification of wood on cutting forces. However, the analysis procedure presented in this work does not allow to conclude quantitatively on the real cutting forces applied on the tool since a strong filtering tends to reduce the measured signal’s amplitude. To do so, more suitable data analysis technics are currently under development.

ACKNOWLEDGEMENTS

Dr. Giacomo Goli would like to acknowledge the ENSAM Cluny for financing one month of staying in Cluny as invited researcher. Rémi Curti would like to acknowledge the COST Action FP1407 for funding a STSM of one week in Florence to work with Dr. Giacomo Goli.

REFERENCES

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Costes J.-P., Ko P.L., Ji T., Decès-Petit C. and Altintas Y. (2004). Orthogonal cutting mechanics of maple: modeling a solid wood-cutting process. Journal of Wood Science,

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de Moura L.F., Brito J.O., Nolasco A.M. and Uliana L.R. (2011). Effect of thermal rectification on machinability of Eucalyptus grandis and Pinus caribaea var. hondurensis woods. European Journal of Wood and Wood Products, 69, 641-648. doi: 10.1007/s00107-010-0507-x.

de Moura Palermo G.P., de Figueiredo Latorraca J.V., de Moura L.F., Nolasco A., Monteiro de Carvalho M. and Rosilei Aparecida G. (2014). Surface roughness of heat treated Eucalyptus grandis wood. Maderas. Ciencia y tecnología, 16. doi: 10.4067/S0718-221X2014005000001.

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Sandak J., Goli G., Cetera P., Sandak A., Cavalli A. and Todaro L. (2017). Machinability of Minor Wooden Species before and after Modification with Thermo-Vacuum Technology. Materials (Basel), 10. doi: 10.3390/ma10020121.

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