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Appendix X X-Ray diffraction patterns

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Appendix X

X-Ray diffraction patterns

1.1 Pristine NC grades

1.1.1 Nanocor® I.30P

Operations: Impor

powder_clay5 - File: nano cpowder_clay5.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Theta:

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 25. 86852 10. 85881

1.1.2 Nanocor® C.30P

Operations: Import

pellets clays sample n°1 - File: pellets_clay_01.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - T

Li n ( C ount s) 0 10000 20000 30000 40000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 54. 73515 22. 18106 11. 10963 7. 21411 6. 29137

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1.1.3 Southern Clay® C15A

p

y

Operations: Import

new powder clay no 02 - File: newclay02.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Theta

Li n ( C ounts ) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 31.338 8 12.52940

1.2 I.30P filled hybrid

1.2.1 7.4i.00pb.02

Operations: Import

I2 : PP + 7.4% NC powder + NO PPgMA - File: i2_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000

Li n ( C ount s) 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100 2200 2300 2400 2500 2600 2700 2800 2900 3000 3100 3200 3300 3400 3500 3600 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 30. 23067 15. 62932 10. 81330 7. 23710 6. 29774

1.2.2 5i.2pb.06

Operations: Import

i6_2 - File: i6_2.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 ° - Theta: 0.500 ° - - Phi: 0.00 ° - -

Lin (C ounts ) 0 1000 2000 3000 4000 5000 6000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 32.7858 4 16.25337 10.61869 7.23710 6.31229

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1.2.3 5i.2pb.07

Operations: Import

PP + 2% PPgMA + 5% powderNC - File: n1_2.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 35.000 ° - Step: 0.040 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - T

Li n (C ount s) 0 1000 2000 3000 4000 5000 2-Theta - Scale 1.52 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 31. 17525 16. 01819 6. 30994 5. 25508 4. 78610 4. 19806 4.06945 3. 50479 3. 12257

1.2.4 5i.5pb.05

Operations: Import

PP + 5% powder NC + 5% PPgMA - File: i3_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Th Operations: Import

I5_1 File: I5_1.raw Type: 2Th/Th locked Start: 1.000 ° End: 15.010 ° Step: 0.030 ° Step time: 1. s Temp.: 25 °C (Room) Time Started: 2 s 2Theta: 1.000 ° Theta: 0.500 ° Phi: 0.00 °

-Lin (

C

ount

s)

0 1000 2000 3000 4000 5000 6000

2-Theta - Scale

1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 33. 58491 15. 90068 10. 41882 6. 32259 33. 55178 16. 02961 6. 29369

1.2.5 5i.5pb.04

Operations: Import

i4 : PP + 5% powderNC + 5% PPgMA - File: i4_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 °

Li n (C ount s) 0 1000 2000 3000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 33. 25043 15. 52176 6. 28766

(4)

1.2.6 5i.5pb.03

Operations: Import

PP + 5% powder NC + 5% PPgMA - File: i3_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Th

Li n ( C ount s) 0 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100 2200 2300 2400 2500 2600 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 33. 30498 15. 92041 6. 30352

1.2.7 5i.20pb.03

Operations: Import

i3 brittle : PP + 5% NC + 20% PPgMA - File: i3_brittle_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1

Li n ( C ount s) 0 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100 2200 2300 2400 2500 2600 2700 2800 2900 3000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 33. 218 9 15. 93603 6. 28493

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1.3 C.30P filled hybrid

1.3.1 13.8c.00pb.01

Operations: Import

C1 after maintenance - File: pelletsC1_after_maintenance.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta

Li n (C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 32. 27679 16. 17280 10. 65312 6. 32269

1.3.2 13.8c.00pb.02

Operations: Import

C2 : PP +13.8% NC dried pellets + NO PPgMA - File: c2_1.RAW - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Thet

Li n (C ount s) 0 100 200 300 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 1800 1900 2000 2100 2200 2300 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 29. 72324 10. 81330

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1.4 C15A filled hybrid

1.4.1 2sc.2pb.04

Operations: Import

L4 2% SC 2% PPgMA - File: L4_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 ° - Theta: 0.500 °

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 37. 73912 20. 86378 14. 28252 10. 24979 6. 31760

1.4.2 2sc.5pb.03

Operations: Import

L3 2% SC 5% PPgMA - File: L3_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Theta: 0.500 °

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 38. 53144 20. 34985 6. 30464

1.4.3 2sc.10pb.07

Operations: Import

L7 2% SC 10% PPgMA - File: L7_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 ° - Theta: 0.500

Lin (C ount s) 0 1000 2000 3000 4000 5000 6000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 40. 39521 21. 46626 6. 31314

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1.4.4 5sc.2pb.05

Operations: Import

L5 5% SC 2% PPgMA - File: L5_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 ° - Theta: 0.500 °

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 32. 77114 13. 75012 6. 32192

1.4.5 5sc.5pb.06

Operations: Import

L6 5% SC 5% PPgMA - File: L6_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 2 s - 2-Theta: 1.000 ° - Theta: 0.500 °

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 11000 12000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 34. 195 3 14. 13019 6. 31384

1.4.6 5sc.15pb.09

Operations: Impor

5 % SC dried 14hrs at 145 C 25 % PPgMA - File: L9_2.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 4 s - 2-Theta: 1.0

Li n ( C ount s) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 37. 9906 2 14. 84194 6. 32270

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1.4.7 5sc.25pb.10

Operations: Import

5 % SC 25 % PPgMA - File: L10_1.raw - Type: 2Th/Th locked - Start: 1.000 ° - End: 15.010 ° - Step: 0.030 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 3 s - 2-Theta: 1.000 ° - Theta: 0.500 °

Li n (Count s) 0 1000 2000 3000 4000 5000 6000 2-Theta - Scale 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1 37.74025 20.11195 6.31348

Riferimenti

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